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The synthesis of nanostructured metal oxides for gas detection is one of the most promising applications of high-energy ball milling. Some significant works have been reported in recent years. Jiang et al. prepared metastable a-Fe 2 O 3 −MO 2 (M: Ti and Sn) solid solutions by high-energy milling for .

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The core/shell nanoparticles were milled and mixed by using a high-power planetary ball mill (Planet M2-3F, Nagao System Inc., Japan). The ball and container were made of partially-stabilized zirconia. The weight ratio of ball to nanoparticles was 40, the speed ratio of rotation to revolution was 2.5, and the revolution speed was 700 rpm.

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Grinding in Ball Mills: Modeling and Process Control

There are three types of grinding media that are commonly used in ball mills: • steel and other metal balls; • metal cylindrical bodies called cylpebs; • ceramic balls with regular or high density. Steel and other metal balls are the most frequently used grinding media with sizes of the balls ranging from 10 to 150 mm in diameter [30].

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